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基于原子荧光光谱法的瓜尔胶中砷和铅的测定

Determination of arsenic and lead in guar gum by atomic fluorescence spectrometry

Modern Analytical Chemistry Research / 2019,1(2): 35-42 / 2019-12-27 755 767

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• Authors: 樊志刚     
• Information:

  山东省化工研究院，济南

• Keywords: 分析化学；瓜尔胶；原子荧光光谱法；氢化物；砷；铅
• Analytical chemistry; Guar gum; Atomic fluorescence spectrometry; Hydride; Arsenic; Lead
• Abstract: 采用氢化物发生 - 原子荧光光谱法测定瓜尔胶中砷和铅，对仪器工作条件和氢 化物发生条件进行选择和优化。方法对砷和铅的检出限均为 0.01μg/L，精密度（RSD， n=6）为 5.94% ～ 10.7%，砷平行加标回收率为 96.5%，铅平行加标回收率为92.9%。
• Arsenic and lead in guar gum were determined by hydride generation - atomic fluorescence spectrometry. Methods the detection limits of arsenic and lead were 0.01 g/L, the precision (RSD, n=6) was 5.94% ~ 10.7%, the recovery rate of arsenic was 96.5%, and that of lead was 92.9%.
• DOI: https://doi.org/10.35534/macr.0102006c
• Cite: 樊志刚．基于原子荧光光谱法的瓜尔胶中砷和铅的测定［J］．现代分析化学研究，2019，1（2）：35-42．